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Calibration parameters SIM TIC p-values
Mean ± 95% CI (n=14) Mean ± 95% CI (n=14)

R² of relative peak area

0.993 ± 0.003

0.97 ± 0.02

0.04

LOD of relative peak area

0.06 ± 0.02

0.07 ± 0.01

0.05

Min LOD

0.04

0.07

 

Max LOD

0.1

0.1

 

R² of relative peak height

0.97 ± 0.01

0.97 ± 0.02

0.93

LOD of relative peak height

0.07 ± 0.03

0.07 ± 0.01

0.4

Min

0.05

0.07

 

Max

0.1

0.1

 

Table 3. Comparison of average R2 values and LOD values of relative peak area and relative peak height of the 14 amino acids in SIM and TIC modes. A matched sample t-test was used to determine the p-values.